Development and validation of an analytical method for the simultaneous determination of benzoylecgonine and ecgonine methyl ester in human urine by gas chromatography/mass spectrometry

A simple and rapid procedure has been developed and validated for the simultaneous determination of benzoylecgonine and ecgonine methyl ester in human urine samples. After extraction and sample cleanup by solid-phase extraction (SPE), the extracts were derivatized with 50 uL of MTBSTFA and analyzed...

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Autores principales: Montes de Oca Porto, Rodny, Correa Vidal, Teresa, Martínez Brito, Dayamín, González Hernández, Sandy, Terrero, Olga L., Granda Fraga, Mario
Formato: Articulo Comunicacion
Lenguaje:Inglés
Publicado: 2010
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Acceso en línea:http://sedici.unlp.edu.ar/handle/10915/7984
http://www.latamjpharm.org/resumenes/29/5/LAJOP_29_5_2_2.pdf
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