Dissolution of nickel oxide in oxalic acid aqueous solutions

The dissolution of nickel oxide (bunsenite) in acid solutions containing oxalic acid has been studied at 70.0°C. The dependencies of the rate of dissolution on total oxalate concentration and on pH have been explained by assuming a mechanism involving the transfer of two different surface complexes,...

Descripción completa

Guardado en:
Detalles Bibliográficos
Autor principal: Figueroa, C.A
Otros Autores: Sileo, E.E, Morando, P.J, Blesa, M.A
Formato: Capítulo de libro
Lenguaje:Inglés
Publicado: Academic Press Inc. 2001
Materias:
PH
Acceso en línea:Registro en Scopus
DOI
Handle
Registro en la Biblioteca Digital
Aporte de:Registro referencial: Solicitar el recurso aquí
LEADER 07161caa a22010337a 4500
001 PAPER-1829
003 AR-BaUEN
005 20230518203109.0
008 190411s2001 xx ||||fo|||| 00| 0 eng|d
024 7 |2 scopus  |a 2-s2.0-0035893793 
024 7 |2 cas  |a nickel, 7440-02-0; oxalic acid, 144-62-7 
040 |a Scopus  |b spa  |c AR-BaUEN  |d AR-BaUEN 
030 |a JCISA 
100 1 |a Figueroa, C.A. 
245 1 0 |a Dissolution of nickel oxide in oxalic acid aqueous solutions 
260 |b Academic Press Inc.  |c 2001 
270 1 0 |m Blesa, M.A.; Unidad de Actividad Química, Centro Atómco Constituyentes, Comision Nacional de Energia Atomica, Avenida Gral Paz 1499, (1650) San Martin, Pcia Buenos Aires, Argentina; email: miblesa@cnea.gov.ar 
506 |2 openaire  |e Política editorial 
504 |a Segall, R.L., Smart, R.St.C., Turner, P.S., (1998) Surface and Near Surface Chemistry of Oxide Materials, , (J. Nowotny and L.-C. Dufour, Eds.). Elsevier, Amsterdam 
504 |a Nii, K., (1970) Corrosion Sci., 10, p. 571 
504 |a Yohe, R., Riga, A., Yeager, E., (1968) Electrochim. Acta, 113, p. 1351 
504 |a Valverde, N., (1976) Ber. Bunsenges. Phys. Chem., 80, p. 333 
504 |a Blesa, M.A., Morando, P.J., Regazzoni, A.E., (1994) Chemical Dissolution of Metal Oxides, , CRC Press, Boca Raton, FL 
504 |a Jones, C.F., Segall, R.L., Smart, R.St.C., Turner, P.S., (1977) J. Chem. Soc. Faraday Trans. I, 73, p. 1710 
504 |a Jones, C.F., Segall, R.L., Smart, R.St.C., Turner, P.S., (1978) J. Chem. Soc. Faraday Trans. I, 74, p. 1615 
504 |a Jones, C.F., Segall, R.L., Smart, R.St.C., Turner, P.S., (1978) J. Chem. Soc. Faraday Trans. I, 74, p. 1624 
504 |a Diggle, J.W., (1973) Oxides and Oxide Films, 2. , J. W. Diggle, Ed. Dekker, New York 
504 |a Ludwig, C., Casey, W.H., (1996) J. Colloid Interf. Sci., 178, p. 176 
504 |a Ludwig, C., Devidal, J.-L., Casey, W.H., (1996) Geochim. Cosmochim. Acta, 60, p. 213 
504 |a Ludwig, C., Casey, W.H., Rock, P.A., (1995) Nature, 375, p. 44 
504 |a Koch, G., (1965) Ber. Bunsen. Phys. Chem., 69, p. 141 
504 |a Data Base from International Center for Diffraction Data (ICDD), PDF 33-0664; Vogel, A.J., (1961) Química Analítica Cuantitativa, 2. , Kapelusz, Buenos Aires 
504 |a Massart, D.L., Vandeginste, B.G.M., Buydens, L.M.C., De Jong, S., Lewi, P.J., Smeyers-Verbeke, J., (1997) Handbook of Chemometrics and Qualimetrics: Part A, , Elsevier, Dordrecht 
504 |a Hug, S.J., Sulzberger, B., (1994) Langmuir, 10, p. 3587 
504 |a Weisz, A.D., (2001), PhD. Diss., to be submitted. University of Buenos Aires, Argentina; Weisz, A.D., Regazzoni, A.E., Blesa, M.A., (2001) Solid State Ionics, 143, p. 125 
504 |a Parfitt, R.L., Farmer, V.C., Russell, J.D., (1977) J. Soil. Sci., 28, p. 29 
504 |a Filius, J.D., Hiemstra, T., Van Riemsdijk, W.H., (1997) J. Colloid Interf. Sci., 195, p. 368 
504 |a Blesa, M.A., Marinovich, H.A., Baumgartner, E.C., Maroto, A.J.G., (1987) Inorg. Chem., 26, p. 3713 
504 |a Borghi, E.B., Morando, P.J., Blesa, M.A., (1991) Langmuir, 7, p. 1652 
504 |a Figueroa, C.A., Sileo, E.E., Morando, P.J., Blesa, M.A., (2000) J. Colloid Interf. Sci., 225, p. 403 
504 |a Vermilyea, D.A., (1966) J. Electrochem. Soc., 113, p. 1067 
504 |a Baumgartner, E.C., Blesa, M.A., Maroto, A.J.G., (1982) J. Chem. Soc., Dalton Trans., p. 1649 
520 3 |a The dissolution of nickel oxide (bunsenite) in acid solutions containing oxalic acid has been studied at 70.0°C. The dependencies of the rate of dissolution on total oxalate concentration and on pH have been explained by assuming a mechanism involving the transfer of two different surface complexes, I and II, that predominate in different pH ranges. The rate law is R = k1 {I} + k2 {II}, where {} denotes surface concentration. The values k1Ns = 3.04 × 10-3 mol Ni m-2 s-1, k2Ns = 1.84 × 10-3 mol Ni m-2 s-1, together with the stability constants K1 = 675 mol-1 dm3 and K2 = 60 mol-1 dm3 fit all the results very well. The species formed in more acidic media is both more stable and more reactive. The possible structures of I and II are discussed on the basis of Fourier transform IR spectroscopy evidence in the literature. © 2001 Elsevier Science.  |l eng 
536 |a Detalles de la financiación: Comisión Nacional de Energía Atómica, Gobierno de Argentina, CNEA 
536 |a Detalles de la financiación: Consejo Nacional de Investigaciones Científicas y Técnicas, PIP 4196 
536 |a Detalles de la financiación: This work was supported by CNEA (Program 5), CONICET (Grant PIP 4196.) and ANPCyT (Grant PICT. 06-00000-00306.). We thank Dr. J. Magallanes for his help. PJM and MAB are members of CONICET. 
593 |a Unidad De Actividad Química, Centro Atómco Constituyentes, Comisión Nacional De Energía Atómica, Avenida Gral Paz 1499, Pcia Buenos Aires, (1650), Argentina 
593 |a INQUIMAE, Facultad De Ciencias Exactas Y Naturales, Universidad De Buenos Aires, Buenos Aires, C1428EHA, Argentina 
593 |a Instituto De Tecnología Prof. J. Sábato, Universidad Nacional De General San Martín, Buenos Aires, Argentina 
593 |a Escuela De Posgrado, Universidad Nacional De General San Martín, Buenos Aires, Argentina 
690 1 0 |a DISSOLUTION 
690 1 0 |a NICKEL OXIDE 
690 1 0 |a OXALIC ACID 
690 1 0 |a SURFACE COMPLEXATION 
690 1 0 |a CARBOXYLIC ACIDS 
690 1 0 |a COMPLEXATION 
690 1 0 |a DISSOLUTION 
690 1 0 |a FOURIER TRANSFORM INFRARED SPECTROSCOPY 
690 1 0 |a PH EFFECTS 
690 1 0 |a SOLUTIONS 
690 1 0 |a STABILITY CONSTANTS 
690 1 0 |a NICKEL COMPOUNDS 
690 1 0 |a NICKEL 
690 1 0 |a OXALIC ACID 
690 1 0 |a AQUEOUS SOLUTION 
690 1 0 |a ARTICLE 
690 1 0 |a COMPLEX FORMATION 
690 1 0 |a CONCENTRATION (PARAMETERS) 
690 1 0 |a DISSOLUTION 
690 1 0 |a FOURIER ANALYSIS 
690 1 0 |a INFRARED SPECTROSCOPY 
690 1 0 |a MOLECULAR STABILITY 
690 1 0 |a PRIORITY JOURNAL 
690 1 0 |a SYNTHESIS 
690 1 0 |a TEMPERATURE DEPENDENCE 
690 1 0 |a TRANSPORT KINETICS 
650 1 7 |2 spines  |a PH 
700 1 |a Sileo, E.E. 
700 1 |a Morando, P.J. 
700 1 |a Blesa, M.A. 
773 0 |d Academic Press Inc., 2001  |g v. 244  |h pp. 353-358  |k n. 2  |p J. Colloid Interface Sci.  |x 00219797  |w (AR-BaUEN)CENRE-15  |t Journal of Colloid and Interface Science 
856 4 1 |u https://www.scopus.com/inward/record.uri?eid=2-s2.0-0035893793&doi=10.1006%2fjcis.2001.7862&partnerID=40&md5=aa060eb5152bf24b5032a552a68c1621  |y Registro en Scopus 
856 4 0 |u https://doi.org/10.1006/jcis.2001.7862  |y DOI 
856 4 0 |u https://hdl.handle.net/20.500.12110/paper_00219797_v244_n2_p353_Figueroa  |y Handle 
856 4 0 |u https://bibliotecadigital.exactas.uba.ar/collection/paper/document/paper_00219797_v244_n2_p353_Figueroa  |y Registro en la Biblioteca Digital 
961 |a paper_00219797_v244_n2_p353_Figueroa  |b paper  |c PE 
962 |a info:eu-repo/semantics/article  |a info:ar-repo/semantics/artículo  |b info:eu-repo/semantics/publishedVersion 
963 |a VARI 
999 |c 62782