A SAXS and swelling study of cured natural rubber/styrene-butadiene rubber blends

A small-angle X-ray scattering (SAXS) and swelling study of natural rubber and styrene-butadiene rubber blends (NR/SBR) is presented. To this aim, specimens of NR and SBR and blends with 75/25, 50/50, and 25/75 NR/SBR ratios (in phr) were prepared at a cure temperature of 433 K and the optimum cure...

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Autor principal: Salgueiro, Walter Alberto
Otros Autores: Somoza, Alberto Horacio, Marzocca, Angel José, Torriani, I., Mansilla, Marcela Angela
Formato: Capítulo de libro
Lenguaje:Inglés
Publicado: 2009
Acceso en línea:Registro en Scopus
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100 1 |a Salgueiro, Walter Alberto 
245 1 2 |a A SAXS and swelling study of cured natural rubber/styrene-butadiene rubber blends 
260 |c 2009 
270 1 0 |m Somoza, A.; IFIMAT-UNCentro, Comisión de Investigaciones Científicas de la Provincia de Buenos Aires, Pinto 399, B7000GHG Tandil, Argentina; email: asomoza@exa.unicen.edu.ar 
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504 |a Marzocca, A.J., Cerveny, S., Salgueiro, W., Somoza, A., Gonzalez, L., (2002) Phys Rev E, 65, pp. 0218011-0218015 
504 |a Salgueiro, W., Marzocca, A.J., Somoza, A., Consolati, G., Cerveny, S., Quasso, F., Goyanes, S., (2004) Polymer, 45, pp. 6037-6044 
504 |a Salgueiro, W., Somoza, A., Torriani, I.L., Marzocca, A.J., (2007) J Polym Sci Part B: Polym Phys, 45, pp. 2966-2971 
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506 |2 openaire  |e Política editorial 
520 3 |a A small-angle X-ray scattering (SAXS) and swelling study of natural rubber and styrene-butadiene rubber blends (NR/SBR) is presented. To this aim, specimens of NR and SBR and blends with 75/25, 50/50, and 25/75 NR/SBR ratios (in phr) were prepared at a cure temperature of 433 K and the optimum cure time (t100). This time was obtained from rheometer torque curves. The system of cure used in the samples was sulfur/n-t-butyl-2-benzothiazole sulfenamide. From swelling tests of the cured samples, information about the molecular weight of the network chain between chemical crosslinks was obtained. For all cured compounds, in the Lorentz plots built from SAXS scattering curves, a maximum of the scattering vector q around 0.14 Å -1 was observed. However, the q position shows a linear-like shift toward lower values when the SBR content in the SBR/NR blend increases. In pure NR or SBR the q values show a different tendency. The results obtained are discussed in terms of the existence of different levels of vulcanization for each single phase forming the blend and the existence of a third level of vulcanization located in the interfacial NR/SBR layer. © 2009 Wiley Periodicals, Inc.  |l eng 
593 |a IFIMAT-UNCentro, Comisión de Investigaciones Científicas de la Provincia de Buenos Aires, Pinto 399, B7000GHG Tandil, Argentina 
593 |a LPMPyMC, Departamento de Física, Ciudad Universitaria, Pabellón I, C1428EGA Buenos Aires, Argentina 
593 |a Instituto de Física Gleb Wataghin, Universidade Estadual de Campinas, CP 6165, 13084-971 Campinas, Sao Paulo, Brazil 
690 1 0 |a BLENDS 
690 1 0 |a NR 
690 1 0 |a RUBBER 
690 1 0 |a RUBBER BLENDS 
690 1 0 |a SAXS 
690 1 0 |a SBR 
690 1 0 |a VULCANIZATION 
690 1 0 |a BENZOTHIAZOLES 
690 1 0 |a BUTADIENE RUBBER 
690 1 0 |a CHEMICAL CROSSLINKS 
690 1 0 |a CURE TEMPERATURE 
690 1 0 |a CURE TIME 
690 1 0 |a LORENTZ 
690 1 0 |a NATURAL RUBBER 
690 1 0 |a NETWORK CHAINS 
690 1 0 |a NR 
690 1 0 |a Q-VALUES 
690 1 0 |a RUBBER BLENDS 
690 1 0 |a SCATTERING CURVE 
690 1 0 |a SCATTERING VECTORS 
690 1 0 |a SINGLE PHASE 
690 1 0 |a SMALL ANGLE X-RAY SCATTERING 
690 1 0 |a STYRENE BUTADIENE RUBBER 
690 1 0 |a SULFENAMIDES 
690 1 0 |a SWELLING STUDIES 
690 1 0 |a SWELLING TEST 
690 1 0 |a THIRD LEVEL 
690 1 0 |a TORQUE CURVES 
690 1 0 |a BUTADIENE 
690 1 0 |a CROSSLINKING 
690 1 0 |a CURING 
690 1 0 |a SCATTERING 
690 1 0 |a STYRENE 
690 1 0 |a VULCANIZATION 
690 1 0 |a X RAY SCATTERING 
690 1 0 |a RUBBER 
700 1 |a Somoza, Alberto Horacio 
700 1 |a Marzocca, Angel José 
700 1 |a Torriani, I. 
700 1 |a Mansilla, Marcela Angela 
773 0 |d 2009  |g v. 47  |h pp. 2320-2327  |k n. 23  |p J Polym Sci Part B  |x 08876266  |w (AR-BaUEN)CENRE-5763  |t Journal of Polymer Science, Part B: Polymer Physics 
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