Fused and unzipped carbon nanotubes, electrochemically treated, for selective determination of dopamine and serotonin
Glassy carbon electrodes (GC) were modified with multiwalled carbon nanotubes (MWCNT/GC) and electrochemically treated first by applying an oxidation potential and then a reduction potential. The resulting electrodes were characterized via scanning electron microscopy, Raman spectroscopy, energy dis...
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Elsevier Ltd
2018
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| 008 | 190410s2018 xx ||||fo|||| 00| 0 eng|d | ||
| 024 | 7 | |2 scopus |a 2-s2.0-85049342090 | |
| 040 | |a Scopus |b spa |c AR-BaUEN |d AR-BaUEN | ||
| 030 | |a ELCAA | ||
| 100 | 1 | |a Bonetto, M.C. | |
| 245 | 1 | 0 | |a Fused and unzipped carbon nanotubes, electrochemically treated, for selective determination of dopamine and serotonin |
| 260 | |b Elsevier Ltd |c 2018 | ||
| 270 | 1 | 0 | |m Bonetto, M.C.; Laboratory of Biosensors and Bioanalysis (LABB), Departamento de Química Biológica e IQUIBICEN-CONICET, Ciudad Universitaria, Facultad de Ciencias Exactas y Naturales, Universidad de Buenos Aires, Intendente Güiraldes 2160, Pabellón 2, Argentina; email: celinatt@yahoo.com.ar |
| 506 | |2 openaire |e Política editorial | ||
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| 520 | 3 | |a Glassy carbon electrodes (GC) were modified with multiwalled carbon nanotubes (MWCNT/GC) and electrochemically treated first by applying an oxidation potential and then a reduction potential. The resulting electrodes were characterized via scanning electron microscopy, Raman spectroscopy, energy dispersive spectroscopy, and electrochemical techniques, particularly cyclic voltammetry using the redox probes Fe(CN)6 3− /4- and Ru(NH3)2+/3+ and electrochemical impedance spectroscopy using Fe(CN)6 3− /4-. These modified electrodes showed an electrochemical determination selective for dopamine (DA) and serotonin (5HT) in the presence of ascorbic acid (AA) and uric acid (UA), simultaneously measured, with a high reproducibility (an RSD of 1.7% for DA and 1.6% for 5HT) and a limit of detection (LOD) of 235 nmol L−1 for DA and 460 nmol L−1 for 5HT. The GC electrodes modified with oxidized MWCNT, subsequently reduced, showed higher selectivity towards the oxidation of DA and 5HT compared with GC bare electrodes or modified with MWCNT or oxidized MWCNT. © 2018 Elsevier Ltd |l eng | |
| 536 | |a Detalles de la financiación: National Council for Scientific Research | ||
| 536 | |a Detalles de la financiación: Universidad de Buenos Aires | ||
| 536 | |a Detalles de la financiación: Inter-American Development Bank, PICT 2014-3407, PICT 2014-0402 | ||
| 536 | |a Detalles de la financiación: Agencia Nacional de Promoción Científica y Tecnológica | ||
| 536 | |a Detalles de la financiación: Consejo Nacional de Investigaciones Científicas y Técnicas, PIP 112-200801-00502 | ||
| 536 | |a Detalles de la financiación: This work was supported by the University of Buenos Aires (IQUIBICEN-CONICET), the National Council for Scientific and Technological Research (CONICET, PIP 112-200801-00502 ), and the ANPCyT (Préstamo BID, PICT 2014-3407 and PICT 2014-0402 ). We also want to thank to Silvia Rodriguez, for editing this manuscript and CONICET Researcher Leonardo Slep for kindly provide us hexaammineruthenium (III) chloride, without his help, the electrochemical characterization of the electrodes with this outer-sphere redox probe would not have been possible. | ||
| 593 | |a Laboratory of Biosensors and Bioanalysis (LABB), Departamento de Química Biológica e IQUIBICEN-CONICET, Ciudad Universitaria, Facultad de Ciencias Exactas y Naturales, Universidad de Buenos Aires, Intendente Güiraldes 2160, Pabellón 2, Ciudad Autónoma de Buenos Aires, C1428EGA, Argentina | ||
| 593 | |a Departamento de Química Inorgánica, Analítica y Química Física, Ciudad Universitaria, Facultad de Ciencias Exactas y Naturales, Universidad de Buenos Aires, Intendente Güiraldes 2160, Pabellón 2, Ciudad Autónoma de Buenos Aires, C1428EGA, Argentina | ||
| 593 | |a DEINSO (Departamento de Investigaciones en Sólidos), UNIDEF-CITEDEF, J.B. de la Salle 4397, (1603) Villa Martelli, Buenos Aires, Argentina | ||
| 593 | |a CONICET, Buenos Aires, Argentina | ||
| 690 | 1 | 0 | |a DOPAMINE |
| 690 | 1 | 0 | |a ELECTROCHEMICAL TREATMENT |
| 690 | 1 | 0 | |a HYBRID FILM |
| 690 | 1 | 0 | |a MULTIWALLED CARBON NANOTUBES |
| 690 | 1 | 0 | |a SEROTONIN |
| 690 | 1 | 0 | |a AMINES |
| 690 | 1 | 0 | |a ASCORBIC ACID |
| 690 | 1 | 0 | |a CHEMICAL DETECTION |
| 690 | 1 | 0 | |a CYCLIC VOLTAMMETRY |
| 690 | 1 | 0 | |a ELECTROCHEMICAL IMPEDANCE SPECTROSCOPY |
| 690 | 1 | 0 | |a ENERGY DISPERSIVE SPECTROSCOPY |
| 690 | 1 | 0 | |a GLASS MEMBRANE ELECTRODES |
| 690 | 1 | 0 | |a NEUROPHYSIOLOGY |
| 690 | 1 | 0 | |a OXIDATION |
| 690 | 1 | 0 | |a SCANNING ELECTRON MICROSCOPY |
| 690 | 1 | 0 | |a YARN |
| 690 | 1 | 0 | |a DOPAMINE |
| 690 | 1 | 0 | |a ELECTROCHEMICAL DETERMINATION |
| 690 | 1 | 0 | |a ELECTROCHEMICAL TECHNIQUES |
| 690 | 1 | 0 | |a ELECTROCHEMICAL TREATMENTS |
| 690 | 1 | 0 | |a GLASSY CARBON ELECTRODES |
| 690 | 1 | 0 | |a HYBRID FILM |
| 690 | 1 | 0 | |a SELECTIVE DETERMINATION |
| 690 | 1 | 0 | |a SEROTONIN |
| 690 | 1 | 0 | |a MULTIWALLED CARBON NANOTUBES (MWCN) |
| 700 | 1 | |a Muñoz, F.F. | |
| 700 | 1 | |a Diz, V.E. | |
| 700 | 1 | |a Sacco, N.J. | |
| 700 | 1 | |a Cortón, E. | |
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