Synthesis of 17a-alkyl- and 17a-aryl-3β-acetoxy- and 3β-methoxy-17a-aza-d-homoandrost-5-en-17-one

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A short and efficient preparation of 17a-methyl-, 17a-ethyl-, 17a-allyl-, and 17a-benzyl-3β-acetoxy-17a-aza-d-homoandrost-5-en-17-one, as well as 17a-methyl-, 17a-ethyl-, and 17a-allyl-3β-methoxy-17a-aza-s-homoandrost-5-en-17-one from the corresponding androsten-17-one derivatives is described. (Ste...

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Autores principales:	Revelli, G.A., Gros, E.G.
Formato:	JOUR
Materias:	17a-aza-d-homoandrost-5-en-17-one derivatives 13C nuclear magnetic resonance spectra 1H nuclear magnetic resonance spectra azasteroids synthesis 17a allyl 3beta acetoxy 17a aza d homoandrost 5 en 17 one 17a allyl 3beta methoxy 17a aza d homoandrost 5 en 17 one 17a benzyl 3beta acetoxy 17a aza d homoandrost 5 en 17 one 17a ethyl 3beta acetoxy 17a aza d homoandrost 5 en 17 one 17a ethyl 3beta methoxy 17a aza d homoandrost 5 en 17 one 17a methyl 3beta acetoxy 17a aza d homoandrost 5 en 17 one 17a methyl 3beta methoxy 17a aza d homoandrost 5 en 17 one 3beta acetoxy 17a aza d homoandrost 5 en 17 one 3beta methoxy 17a aza d homoandrost 5 en 17 one azasteroid unclassified drug article carbon nuclear magnetic resonance drug structure drug synthesis mass spectrometry proton nuclear magnetic resonance Androstenols Azasteroids Magnetic Resonance Spectroscopy Molecular Structure Support, Non-U.S. Gov't
Acceso en línea:	http://hdl.handle.net/20.500.12110/paper_0039128X_v58_n4_p181_Revelli
Aporte de:	Biblioteca Digital - Facultad de Ciencias Exactas y Naturales (UBA) de Universidad de Buenos Aires

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spelling	todo:paper_0039128X_v58_n4_p181_Revelli2023-10-03T14:49:21Z Synthesis of 17a-alkyl- and 17a-aryl-3β-acetoxy- and 3β-methoxy-17a-aza-d-homoandrost-5-en-17-one Revelli, G.A. Gros, E.G. 17a-aza-d-homoandrost-5-en-17-one derivatives 13C nuclear magnetic resonance spectra 1H nuclear magnetic resonance spectra azasteroids synthesis 17a allyl 3beta acetoxy 17a aza d homoandrost 5 en 17 one 17a allyl 3beta methoxy 17a aza d homoandrost 5 en 17 one 17a benzyl 3beta acetoxy 17a aza d homoandrost 5 en 17 one 17a ethyl 3beta acetoxy 17a aza d homoandrost 5 en 17 one 17a ethyl 3beta methoxy 17a aza d homoandrost 5 en 17 one 17a methyl 3beta acetoxy 17a aza d homoandrost 5 en 17 one 17a methyl 3beta methoxy 17a aza d homoandrost 5 en 17 one 3beta acetoxy 17a aza d homoandrost 5 en 17 one 3beta methoxy 17a aza d homoandrost 5 en 17 one azasteroid unclassified drug article carbon nuclear magnetic resonance drug structure drug synthesis mass spectrometry proton nuclear magnetic resonance Androstenols Azasteroids Magnetic Resonance Spectroscopy Molecular Structure Support, Non-U.S. Gov't A short and efficient preparation of 17a-methyl-, 17a-ethyl-, 17a-allyl-, and 17a-benzyl-3β-acetoxy-17a-aza-d-homoandrost-5-en-17-one, as well as 17a-methyl-, 17a-ethyl-, and 17a-allyl-3β-methoxy-17a-aza-s-homoandrost-5-en-17-one from the corresponding androsten-17-one derivatives is described. (Steroids 58:181-184, 1993). © 1993. Fil:Revelli, G.A. Universidad de Buenos Aires. Facultad de Ciencias Exactas y Naturales; Argentina. Fil:Gros, E.G. Universidad de Buenos Aires. Facultad de Ciencias Exactas y Naturales; Argentina. JOUR info:eu-repo/semantics/openAccess http://creativecommons.org/licenses/by/2.5/ar http://hdl.handle.net/20.500.12110/paper_0039128X_v58_n4_p181_Revelli
institution	Universidad de Buenos Aires
institution_str	I-28
repository_str	R-134
collection	Biblioteca Digital - Facultad de Ciencias Exactas y Naturales (UBA)
topic	17a-aza-d-homoandrost-5-en-17-one derivatives 13C nuclear magnetic resonance spectra 1H nuclear magnetic resonance spectra azasteroids synthesis 17a allyl 3beta acetoxy 17a aza d homoandrost 5 en 17 one 17a allyl 3beta methoxy 17a aza d homoandrost 5 en 17 one 17a benzyl 3beta acetoxy 17a aza d homoandrost 5 en 17 one 17a ethyl 3beta acetoxy 17a aza d homoandrost 5 en 17 one 17a ethyl 3beta methoxy 17a aza d homoandrost 5 en 17 one 17a methyl 3beta acetoxy 17a aza d homoandrost 5 en 17 one 17a methyl 3beta methoxy 17a aza d homoandrost 5 en 17 one 3beta acetoxy 17a aza d homoandrost 5 en 17 one 3beta methoxy 17a aza d homoandrost 5 en 17 one azasteroid unclassified drug article carbon nuclear magnetic resonance drug structure drug synthesis mass spectrometry proton nuclear magnetic resonance Androstenols Azasteroids Magnetic Resonance Spectroscopy Molecular Structure Support, Non-U.S. Gov't
spellingShingle	17a-aza-d-homoandrost-5-en-17-one derivatives 13C nuclear magnetic resonance spectra 1H nuclear magnetic resonance spectra azasteroids synthesis 17a allyl 3beta acetoxy 17a aza d homoandrost 5 en 17 one 17a allyl 3beta methoxy 17a aza d homoandrost 5 en 17 one 17a benzyl 3beta acetoxy 17a aza d homoandrost 5 en 17 one 17a ethyl 3beta acetoxy 17a aza d homoandrost 5 en 17 one 17a ethyl 3beta methoxy 17a aza d homoandrost 5 en 17 one 17a methyl 3beta acetoxy 17a aza d homoandrost 5 en 17 one 17a methyl 3beta methoxy 17a aza d homoandrost 5 en 17 one 3beta acetoxy 17a aza d homoandrost 5 en 17 one 3beta methoxy 17a aza d homoandrost 5 en 17 one azasteroid unclassified drug article carbon nuclear magnetic resonance drug structure drug synthesis mass spectrometry proton nuclear magnetic resonance Androstenols Azasteroids Magnetic Resonance Spectroscopy Molecular Structure Support, Non-U.S. Gov't Revelli, G.A. Gros, E.G. Synthesis of 17a-alkyl- and 17a-aryl-3β-acetoxy- and 3β-methoxy-17a-aza-d-homoandrost-5-en-17-one
topic_facet	17a-aza-d-homoandrost-5-en-17-one derivatives 13C nuclear magnetic resonance spectra 1H nuclear magnetic resonance spectra azasteroids synthesis 17a allyl 3beta acetoxy 17a aza d homoandrost 5 en 17 one 17a allyl 3beta methoxy 17a aza d homoandrost 5 en 17 one 17a benzyl 3beta acetoxy 17a aza d homoandrost 5 en 17 one 17a ethyl 3beta acetoxy 17a aza d homoandrost 5 en 17 one 17a ethyl 3beta methoxy 17a aza d homoandrost 5 en 17 one 17a methyl 3beta acetoxy 17a aza d homoandrost 5 en 17 one 17a methyl 3beta methoxy 17a aza d homoandrost 5 en 17 one 3beta acetoxy 17a aza d homoandrost 5 en 17 one 3beta methoxy 17a aza d homoandrost 5 en 17 one azasteroid unclassified drug article carbon nuclear magnetic resonance drug structure drug synthesis mass spectrometry proton nuclear magnetic resonance Androstenols Azasteroids Magnetic Resonance Spectroscopy Molecular Structure Support, Non-U.S. Gov't
description	A short and efficient preparation of 17a-methyl-, 17a-ethyl-, 17a-allyl-, and 17a-benzyl-3β-acetoxy-17a-aza-d-homoandrost-5-en-17-one, as well as 17a-methyl-, 17a-ethyl-, and 17a-allyl-3β-methoxy-17a-aza-s-homoandrost-5-en-17-one from the corresponding androsten-17-one derivatives is described. (Steroids 58:181-184, 1993). © 1993.
format	JOUR
author	Revelli, G.A. Gros, E.G.
author_facet	Revelli, G.A. Gros, E.G.
author_sort	Revelli, G.A.
title	Synthesis of 17a-alkyl- and 17a-aryl-3β-acetoxy- and 3β-methoxy-17a-aza-d-homoandrost-5-en-17-one
title_short	Synthesis of 17a-alkyl- and 17a-aryl-3β-acetoxy- and 3β-methoxy-17a-aza-d-homoandrost-5-en-17-one
title_full	Synthesis of 17a-alkyl- and 17a-aryl-3β-acetoxy- and 3β-methoxy-17a-aza-d-homoandrost-5-en-17-one
title_fullStr	Synthesis of 17a-alkyl- and 17a-aryl-3β-acetoxy- and 3β-methoxy-17a-aza-d-homoandrost-5-en-17-one
title_full_unstemmed	Synthesis of 17a-alkyl- and 17a-aryl-3β-acetoxy- and 3β-methoxy-17a-aza-d-homoandrost-5-en-17-one
title_sort	synthesis of 17a-alkyl- and 17a-aryl-3β-acetoxy- and 3β-methoxy-17a-aza-d-homoandrost-5-en-17-one
url	http://hdl.handle.net/20.500.12110/paper_0039128X_v58_n4_p181_Revelli
work_keys_str_mv	AT revelliga synthesisof17aalkyland17aaryl3bacetoxyand3bmethoxy17aazadhomoandrost5en17one AT groseg synthesisof17aalkyland17aaryl3bacetoxyand3bmethoxy17aazadhomoandrost5en17one
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Synthesis of 17a-alkyl- and 17a-aryl-3β-acetoxy- and 3β-methoxy-17a-aza-d-homoandrost-5-en-17-one

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