Synthesis of |24‐14C|‐3β,14β,20ε‐trihydroxy‐23‐nor‐5β‐cholanoic acid

The synthesis of |24‐14C|‐3β,14β,20ε‐trihydroxy‐23‐nor‐5β‐cholanoic acid was accomplished by Reformatsky reaction of ethyl |1‐14C|‐bromo acetate with 3β‐acetoxy‐14β‐hydroxy‐5β‐pregnan‐20‐one which was obtained from digitoxigenin. The final and intermediate products were characterized by spectroscopi...

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Autores principales: Maier, M.S., Seldes, A.M., Gros, E.G.
Formato: JOUR
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Acceso en línea:http://hdl.handle.net/20.500.12110/paper_03624803_v22_n8_p833_Maier
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